1 Scope
This European Standard describes a method for the determination of calcium, copper,
iron, magnesium, manganese, phosphorus, potassium, sodium, sulfur and zinc in different
foodstuffs using optical emission spectrometry with inductively coupled plasma (ICP-OES)
after pressure digestion.
This method has been validated in an interlaboratory study according to ISO 5725 [1] on infant formula soya based, cheese, chicken meat, wheat flour, apple juice,
lobster and milk (see elements ranges Table 1 and validation data in Annex B).
HorRat values greater than 2 have been observed for certain analyte/matrix combinations
during the validation study.
Table 1
—
Validated element ranges
| Element |
Range
mg/kg
|
|---|---|
| Calcium | 70 to 7178 |
| Copper | 0,60 to 16,40 |
| Iron | 0,88 to 77 |
| Magnesium | 45 to 1 174 |
| Manganese | 0,44 to 5,12 |
| Phosphorus | 72 to 9 708 |
| Potassium | 605 to 14 312 |
| Sodium | 11 to 2 220 |
| Sulfur | 26 to 8 542 |
| Zinc | 0,16 to 43,5 |
At European or International level, vertical standards for the determination of specific
minerals can exist, e.g. for milk and milk products or for animal and vegetable fats
and oils [2].